<div class="csl-bib-body">
<div class="csl-entry">MANOUSI, N., Alexandra Beina, Kabir, A., Furton, K. G., Rosenberg, E. E., Zachariadis, G. A., & Kalogiouri, N. P. (2024, May 16). <i>A magnet-integrated fabric phase sorptive extraction protocol as a front-end to GC-MS/MS for the determination of 16 polycyclic aromatic hydrocarbons in water samples</i> [Poster Presentation]. ASAC Junganalytiker:innen Forum 2024, Graz, Austria. http://hdl.handle.net/20.500.12708/209585</div>
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dc.identifier.uri
http://hdl.handle.net/20.500.12708/209585
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dc.description.abstract
Polycyclic aromatic hydrocarbons (PAHs) are hydrophobic organic contaminants that can pollute aquatic and terrestrial species. Due to their mutagenic or carcinogenic properties, 16 PAHs have been classified as priority environmental pollutants by the Environmental Protection Agency (EPA) of the United States. Thus, the determination of these compounds at trace levels in water samples is of utmost importance. Methods: In this work, a magnet-integrated fabric phase sorptive extraction (MI-FPSE) protocol was developed and combined with gas chromatography-tandem mass spectrometry (GC-MS/MS). MI-FPSE is a recently introduced sample preparation approach that integrates the stirring and extraction mechanisms into a single sample preparation device. The main parameters that affect the performance of the MI-FPSE procedure were studied and the analytical method was validated and used for real sample analysis. Results: Sol-gel poly(tetrahydrofuran) MI-FPSE media provided the highest extraction efficiency towards the majority of the target analytes. Under optimum conditions, the LOQs for the target analytes were down to 0.01 μg L-1. Moreover, the sol-gel coated MI-FPSE membranes were found to be reusable in accordance with the requirements of green sample preparation. Conclusions: The MI-FPSE method exhibited good accuracy and precision, wide linear range, and sensitivity. Among the benefits of this procedure are its operational simplicity, high sample throughput, and rapid extraction kinetics. The overall protocol exhibited good method applicability and green merits. Thus, MI-FPSE serves as a highly versatile “all-in-one” technique for the determination of pollutants in environmental samples.
en
dc.language.iso
en
-
dc.subject
FPSE
en
dc.subject
PAHs
en
dc.subject
GC-MS/MS
en
dc.title
A magnet-integrated fabric phase sorptive extraction protocol as a front-end to GC-MS/MS for the determination of 16 polycyclic aromatic hydrocarbons in water samples
en
dc.type
Presentation
en
dc.type
Vortrag
de
dc.contributor.affiliation
TU Wien, Austria
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dc.contributor.affiliation
Aristotle University of Thessaloniki, Greece
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dc.contributor.affiliation
Florida International University, United States of America (the)
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dc.contributor.affiliation
Florida International University, United States of America (the)
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dc.contributor.affiliation
Aristotle University of Thessaloniki, Greece
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dc.contributor.affiliation
Aristotle University of Thessaloniki, Greece
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dc.type.category
Poster Presentation
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tuw.researchTopic.id
M5
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tuw.researchTopic.id
X1
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tuw.researchTopic.name
Composite Materials
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tuw.researchTopic.name
Beyond TUW-research focus
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tuw.researchTopic.value
50
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tuw.researchTopic.value
50
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tuw.publication.orgunit
E164-01-2 - Forschungsgruppe Oberflächen-, Spurenanalytik und Chemometrie
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tuw.author.orcid
0000-0002-1516-8012
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tuw.event.name
ASAC Junganalytiker:innen Forum 2024
en
tuw.event.startdate
16-05-2024
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tuw.event.enddate
17-05-2024
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tuw.event.online
On Site
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tuw.event.type
Event for scientific audience
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tuw.event.place
Graz
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tuw.event.country
AT
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tuw.event.presenter
MANOUSI, NATALIA
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wb.sciencebranch
Chemie
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wb.sciencebranch.oefos
1040
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wb.sciencebranch.value
100
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item.cerifentitytype
Publications
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item.languageiso639-1
en
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item.fulltext
no Fulltext
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item.openairetype
conference poster not in proceedings
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item.openairecristype
http://purl.org/coar/resource_type/c_18co
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item.grantfulltext
none
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crisitem.author.dept
E164-01-2 - Forschungsgruppe Oberflächen-, Spurenanalytik und Chemometrie
-
crisitem.author.dept
Aristotle University of Thessaloniki
-
crisitem.author.dept
Florida International University
-
crisitem.author.dept
Florida International University
-
crisitem.author.dept
E164-01-2 - Forschungsgruppe Oberflächen-, Spurenanalytik und Chemometrie
-
crisitem.author.dept
Aristotle University of Thessaloniki
-
crisitem.author.dept
Aristotle University of Thessaloniki
-
crisitem.author.parentorg
E164-01 - Forschungsbereich Imaging und Instrumentelle Analytische Chemie
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crisitem.author.parentorg
E164-01 - Forschungsbereich Imaging und Instrumentelle Analytische Chemie
