Roshangias, A., Bernardi, J., & Ipser, H. (2016). An attempt to synthesize Sn-Zn-Cu alloy nanoparticles. Materials Letters, 178, 10–14. https://doi.org/10.1016/j.matlet.2016.04.192
E057-02 - Fachbereich Universitäre Serviceeinrichtung für Transmissions- Elektronenmikroskopie
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Journal:
Materials Letters
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ISSN:
0167-577X
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Date (published):
1-Sep-2016
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Number of Pages:
5
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Peer reviewed:
Yes
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Keywords:
Nanoparticles; Sn-Zn-Cu; Core-shell structure; Chemical reduction
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Abstract:
Investigations on the synthesis of bi- or tri-metallic alloy nanoparticles have been relatively limited. Thus, we present here results of experiments to synthesize Sn-30Zn-10Cu (wt%) nanopowder alloys by chemical reduction. Characterization by electron microscopy and powder X-ray diffraction showed that nanoparticles with an average diameter of 20 nm were obtained. Microstructure and phase evolution of the as-synthesized particles upon heating were investigated and compared with the corresponding bulk alloy. The results showed that the nanoparticles contain all three constituents (i.e. Sn, Zn and Cu), possess a core-shell morphology and exhibit a phase configuration different from the bulk alloy.
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Research Areas:
Surfaces and Interfaces: 50% Materials Characterization: 50%